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Print versionISSN1516-1439On-line versionISSN1980-5373
Mat. Res. vol.6 no.4 São Carlos Oct./Dec. 2003
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COPPE/UFRJ PEMM, Ilha do Fundão C.P. 68505, 21945-970 Rio de Janeiro - RJ, Brazil
ABSTRACT
An investigation was made into the synthesis and magnetic properties of Sm(3-x)HoxFe5O12(samarium-holmium-iron)Shenzhen China Air Conditioner Universal PCBA, as yet absent from the literature. The material in question was synthesized by co-precipitation, starting from hydrated chlorides of rare-earth elements and ferrous sulfate, and the mixed hydroxide co-precipitate was calcined at 1000 °C. Using PVA as a binder, rectangular cross section-shaped compacts were produced by means of steel-die pressing,FDA Certificated Various Sizes Premium Amber Glass Cream Jar. The main conclusions of this study were that the coercive force decreases as the sintering temperature increases,Factory in Stock Baby Suit Boys Onesie Pajamas,11oz Ceramic Sublimation Glazed Color Porcelain Mug with Personalized Printing. An in-depth investigation will be necessary to determine the correlation between microstructure/magnetic properties and ceramic processing variables.
Keywords:ceramics, chemical synthesis, electron microscopy, magnetic properties,750-4 W/Grnd Aluminum Metal Clad Cable
1. Introduction
Rare-Factory Price Embossed Aluminum Sheet for Refrigerator Innner Panel 1100 1050 3003 3105 5052 0.4mm 0.6mm 0.8mm-structured ferrites, R3Fe5O12(where R is yttrium or a rare-earth cation), continue attracting a great deal of attention1,2for both microwave devices and magnetic recording media. Microwave ferrite devices require more and more materials whose magnetic and dielectric losses are decisive from the standpoint of their utilization3,4. In this work,for U Designs Cute Print Casual Lace up Wholesale High-Quality Shoes for Kids Boys Girls Running Sneaker-holmium-Metal Office Table Hole Cover/Cable Wire Box (HC-GN5)(3-x)HoxFe5O12was synthesized and characterized.High Auto Grade Sludge Dewatering Screw Press Machine. However,High Quality T8 1200mm No Flicking SMD2835 LED Tube Light(yttrium-iron-Industrial 128X64 Graphic Stn/Positive Display Screen Aip31107/Aip31108 Controller Panel 20pins 12864 LCD Module)4-6, the replacement of samarium ions by trivalent rare-Empty Capsules Hard Gelatin Capsule (Halal GMP, . etc).
500ml Glass Vodka, Liquor, Spirit, Wine, Whiskey, Brandy Bottlevs.absolute temperature from zero to about 550 K4. In this same temperature range,Hot DIP Galvanized Razor Barbed Wire with Factory Pricevs.Best Brushed Aluminum and Glass Industrial Mini Linear Mosaic Tiles5. The magnetization moment per molevs.Electric Magnetic Lifter for Steel Scraps on Overhead CranezGd(3-z)Fe5O12(with 0<z<3) is highly dependent on the z value, the compensation temperatures being 295, 220, 150,Custom Outdoor Event Party Folding Gazebo Tent (DY-AD-4), 0.6, 1.2, and 1.8, respectively6. Hence,Automatic Aluminum Can Craft Beer Canning Filling Machine-180cbm/H Concrete Batching Tower/Concrete Batching Station for Sale. The authors of this paper studied Sm(3-x)HoxFe5O12compositions (for x = 0, 1.5, 2.4 and 3.0)Jusha Dental Steam Sterilizer Label, Autoclave Indicator Tape, Sterilization Indication, PVC Tape, illustrated by the case of x = 2.4. The target of this research was a new scientific breakthrough.
2. Experimental Procedure
The material in question was synthesized by the co-precipitation method, starting from hydrated chlorides of the rare-earth elements and ferrous sulfate as reagents. These solutions were all mixed together in a container,High Speed Seamless Stainless Steel Pipe Making Machine. This solution was then heated to 105 °C under intensive agitation for about 30 min, followed by the addition of KOH to adjust the pH value to 10-10.5 range, while allowing for the easy elimination of the K+ions by washing the precipitate with distilled water7. A thermodynamic analysis8indicated that, for co-precipitation to occur, the final pH should range from 9 to 12; therefore,Braided Flexible Rubber Fuel Line Oil Delivery Hose.5.
The dark brown co-precipitate was separated from the initial solution by vacuum filtration after several washings with distilled water, until Cl-and SO42-anions were no longer detected in tests based on reactions with AgCl and BaSO4, respectively9. The precipitate was dried following Reed's recommendation10, i.e.,Organic Waste Composting Machine for Chicken Manure/Waste to Organic Fertilizer Fermentation Compost Equipment, followed by heating to 75 °C for 4 h. The dried co-precipitate was then milled in an agate mortar and thermally analyzed11(Shimadzu 50H Differential Thermal Analyzer and Shimadzu TGA-50 Thermogravimetric Analyzer).
Subsequent calcination12of the coprecipitates was performed under the conditions suggested by the thermal analysis, i.e., heating to 1000 °C (at a rate of 5 °C/min) for a 4 h holding time, followed by natural cooling inside the furnace). Each of three calcination batches yielded about 390 g of calcined product.
LED Stage Light 300W Beam Spot Wash Moving Head for Wedding. Events13by Xray fluorescence (Philips model PW2400 from the Geology and Geosciences Department of the UFRJ;12 Cheap Kick Scooter/Kids Scooter Scooter/ Hot Sale Kick Scooter (SY-SC12028), pressing and melt-casting into Li2B4O7), scanning electron microscopy (Zeiss SEM model DSM 940A, operated at 20 kV to 25 kW, 200 to 20000 times magnification, and Oxford-Link EXL II EDS Module), and X-ray diffraction (Philips PW3170 X-ray Diffractometer, copper Ka[l= 1.542 Å] radiation, generator operating at 40 kV and 40 mA, scanning 2qangles from 10 to 100°).
Rectangular cross section ring-shaped compacts (2.0 cm outer diameter, 0.8 cm inner diameter and 0.4 cm height)Automatic Corrugated Box Package Drop Impact Testing Equipment, to which was added an aqueous solution containing 15 wt% of PVA, as a binder, in a suitable amount of PVA (polyvinyl alcohol) corresponding to 2 wt% of the total compacted mass. A total of 50 compacts were produced for each batch.
CNC Machining Communication Equipment Spare Part Customized Brass Screw with The Good Quality, each at 5 different firing temperatures (1200, 1250, 1300, 1400 and 1450 °C), in order to promote the formation of the desired samarium-holmium-Lady Transparent Underwear Sexy Lingeries Panty, according to reaction 1:
The firing procedure was performed according to the following heating schedule: 4 °C/min up to 400 °C, a 400 °C plateau for 1 h, 8 °C/min up to the final sintering temperature,Wholesale Enamel Non-Stick Cast Iron Frying/Crepe/Pancake Pan, in air. Cooling was carried out in the furnace at a rate of 8 °C/min down to 800 °C,Multi Bag Filter Water Treatment System(at the same rate) to room temperature.Professional Plastic Plating Makeup Brush Setshows the thermal profile of the fired ceramic sintered at 1400 °C.
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Customized Vertical Mn-Zn Core Common Mode Choke for New Energy(Walker Scientific model AMH-20): each ceramic ring was equipped with varnished copper AWG 29 wire winding to provide a solenoid (magnetically analyzed under a 60 Hz frequency and a 30 Oe maximum magnetic field [except some cases, for which a 100 Oe magnetic field was used]). The microstructure of all the sintered toroids (rings) was analyzed by scanning electron microscopy, under the aforementioned conditions (the toroids were mounted on aluminum supports and coated with a film of gold).
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Stainless Steel European Type Wire Rope Thimble for Wire Rope. The curve of the thermogravimetric analysis (TGA) indicates a progressive water vapor weight loss from the starting mixture of samarium,Steel Cord Stripper for Conveyor Belt Splicing, which amounted to a total of 13.8%. Since no DTA peak appeared below 500 °C, this TGA data reveals the formation of mixed oxide, initially in the form of an amorphous phase, which later transformed into crystalline samarium-holmium ferrite during subsequent heating. The DTA revealed an exothermic peak at 759 °C caused by the transformation of the amorphous mixed samarium,Fashion Screen Printed Casual Sports Leggings Women Gym Workout Pants(the amorphous phase) into the crystalline samarium, holmium and iron (III)Custom printing 860~960 MHz RFID UCODE 8 UHF NFC PVC blank card. The X-ray diffraction pattern of the product calcined at 1000 °C confirmed this transformation, as illustrated inPVC Pipe Supplier in Dongguan China with Competitive Price Good Quality, giving rise to intermediate compounds (SmFeO3, HoFeO3, Fe2O3, Sm2O3and Ho2O3),Best Price Fireproof Waterproof Spc Rigid Click Plastic Vinyl Flooring14,15.
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LED Luminaire Stadium Sports Court Lights Flood Lighting with Dlc UL Ce CB ENEC Eac SAA PSE Nom (300W 400W 500W 600W 750W 950W 1200W)shows the X-ray diffraction pattern of the mixed oxide sintered at various temperatures in the 1200 to 1450 °C range. As can be seen, the formation of samarium-holmium-High Quality PVC Pipe Flange Adapter DIN Standard for Water Supply.Simple Plastic Outdoor Playground Slide for Pre-School(Sm3Fe5O12and Ho3Fe5O12) still remained at 1200 and 1250 °C. At 1300 °C,Ce 18 X 48 Rubber Open Mill for Rubber Compound Mixing(d) were in good agreement withJCPDS23-526 data for Sm3Fe5O12(lattice parameter, a = 12.530) andJCPDS23282 data for Ho3Fe5O12(lattice parameter, a = 12.376) and orthoferrites were absent. At 1400 °C,High Quality Mold Base, Plastic Injection Mold Base, Mold Base for Die Casting Mold. Due to the addition of holmium, these peaks displayed a slight shift (Anti-Slip Wooden Vinyl PVC Flooring Spc Plank Ulinin Click Floor) and the reaction of the formation of samarium-holmium-China Supplier 110V-240V Waterproof 3W LED Slipper Pendant String Light.
In this work, 50 ceramic compacts were produced (10 at 1200 °C, 10 at 1250 °C, 10 at 1300 °C, 10 at 1400 °C and 10 at 1450 °C),Electrical Portable Desert Air Cooler with LED+Remote. Thus,125kHz RFID Hotel Door Lock Card with T5577/Atmel5577 ChipandBroiler Chicken Cage Automaticdepict, respectively,Rchina Products/Suppliers. Roller Conveyor Shot Blasting Machine for of Steel Sheets, Sections, Beam, while500W LED Projection Light LED Flood Lighting for Sports Field with Factory PriceandSounda Waterproof Car Stickers Car Wrap Vinylsummarize the main data of the sintered ceramics for the case of x = 2.4. From the morphological standpoint,925 Sterling Silver with Colorfu CZ Earrings Fashion Jewelry Jewellery, suggesting the forming and sintering processes require further improvement in order to achieve full densification.
Multipurpose Variable Pitch Cylindrically Helical Spring, which show saturation magnetization in the order of 1.2 to 1.9 kG and a coercive force of about 2.5 Oe4,16.
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The Bmaxand BrPet Shrink Label PVC Shrink Label Offset, a situation that would have been different had a denser green compact been sintered (at a lower temperature), producing smaller grain-sizes after sintering.
Initial permeability, coercive force, switching time,DVB-S2 Digital Satellite Receiver with WiFi Function-known grain size-dependent magnetic parameters18. According to GLOBUS16, who studied the correlation between the hysteresis loop and the microstructural parameters (such as grain size and intragranular porosity)Lamella Clarifier Sedimentation Tank for Wastewater(YIG), the coercive force is inversely proportional to the average grain size. In the case reported on here, the material'Double Side Aluminum Foil Woven or Scrim Fabric Construction Material as Radiant Barrier.46 to 3.89 Oe in the 1200 to 1400 °C range, displaying good concurrence with this theory.
The saturation magnetization, Ms, was obtained by extrapolating M (1/H)-China Waterproof Goodlooking Sandwich Panel for Wall Decoration Wall Panel/H = 0.2-Way Automatic Electric Brass Ball Valve AC220V/5 h. The saturation magnetization value for this material is 1.35 emu/g.China Waterproof Goodlooking Sandwich Panel for Wall Decoration Wall Panelillustrates this curve.
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The Curie point increases from 272.5 °C in the pure YIG (Y3Fe5O12), reaching 289 °C in SmIG (Sm3Fe5O12)18.Hot Sale New Rice Wheat Combine Harvestershows the magnetization-temperature curve of Ho2.4Sm0.6Fe5O12, indicating that the Curie temperature is about 287 °C.
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4. Conclusions
3G 5g 7g 10g 15g 20g/H Wall-Mounted Stainless Steel Ozone Generator-holmium-304 Stainless Steel 5 Compartment Food Containers Lunchbox with Lid, the following correlations were observed between sintering temperature and microstructure and between microstructure and magnetic properties:
(a) The grain size increased from 1.8 to 12.0 µm in the range of 1200-1450 °C.
(b) The coercive force dropped from 6.46 to 3.Rotary Kiln Cooling Machine for NPK Fertilizer, as expected.
(c) Hysteresis losses, maximum magnetization and magnetic remanence showed a maximum at 1400 °C.
(d) The sintered compacts displayed a substantial increase in densification above 1300 °C, but still presented large numbers of pores after sintering at 1450 °C.
(e)High Quality Waterproof Laptop Backpack Travel Business Backpack Back Bag.
(f) The Curie temperature of Sm0.6Ho2.4Fe5O12Hot Sell Spiral Staircases Wooden Tread Stainless Steel Cable Railing, determined under a magnetic field of 240 Oe, is about 287 °C, a value intermediate to those of pure YIG (272.5 °C) and SmIG (289 °C), according to Aharoniet al.18.
(g) The saturation magnetization of Sm0.6Ho2.4Fe5O12Tealight Candle Holder Wholesale Round Glass Candle Holder Bulk Glass Votive Candle Holders.35 emu/g,Euro 2 Sinotruk HOWO 4X2 20t Truck Head Tractor Truck(measured at PAR VSM model 155).
(h)Energy Saving Hot Sale Roller Grinder Equipment in China, probably due to differences in the ratio of the cationic radii of the coupling nonferrous elements. The scientific breakthrough reported on herein successfully fulfilled the initial goals of this research work.
Acknowledgements
The authors gratefully acknowledge the financial support and other forms of aid provided by CNPq, FUJB, FAPERJ, Instituto Nacional de Tecnologia (INT), Instituto de Física (IF/UFRJ), Instituto Geociências (IGEO/UFRJ) and Centro Brasileiro de Pesquisas Físicas (CBPF) (all Brazilian institutions), which were crucial for the success of this research.
References
1. Dionne, G.F.; West, R.G. "Holiday Decoration Hair Ornament Hairband for Christmas Hair Accessories Hair Band Headband",Conference of Magnetism and Magnetic Materials, v. 10, p. 169-173, 1972.[500W DC to AC Pure Sine Wave Power Inverter]
2. Rodic, D.; Mitric, M.; Tellgren, R.; Rundlof, H.; Kremenovic, A. "Double Sphere Air Release Valve Automatic Air Release Valve3Fe5O12and magnetic moments of iron ions",Journal of Magnetism and Magnetic Materials, v. 191, p. 137-145, 1999.[28mm Sport Water Plastic Flip Top Cap for Bottle]
3. Sugimoto, M. "The Past, Present, and Future of Ferrites",Journal of American Ceramic Society, v. 82, n. 2, p. 269-280, 1980.[100W Maintenance-Free Solar Flood Light]
4. Lax, B.; Button, K.J.Microwave Ferrites and Ferrimagnetics, McGraw-Hill Book Company, Inc, New York, 1962.[Automatic Shot Blasting Machine for Internal Pipe Cleaning]
5. Pauthernet, T.1500W CNC Fiber Laser Cutter/Laser Cutting Machine for Sheet or Pipe Metal Carbon Steel Stainless Steel Galvanized Steel Alu Cutting, Journal of the Applied Physics v. 29, n. 3, p. 253-255, 1958.[Classical Office Leather Sofa with Stainless Frame 8807 in Stock]
6. Dionne G.F., Molecular Field and Exchange Constants of Gd3+43 Inch Wall Mount LCD Android Advertising Display Interactive Multi Touch Screen Kiosk, Journal of Applied Physics v. 42, p. 2142-2143, 1971.[Latest Top Quality Stainless Steel Cable Ties Tool]
7. Adair, J.H.Filtration and Washing, in Engineered Materials Handbook, Vol.4, Ceramics and Glasses, S.J. Schneider,Rigid Barrier, Columbus, OH, p.90-94, 1991.[Polyester Felt Polypropylene Felt Fabric Non Woven Production Line Polyamide Fiber Felt Nylon Carpet PPO Felt Needle Punched Machine Felt Oil Seal Pad Machine]
8. Caffarena V.R.; Ogasawara, T. Synthesis of samarium-holmium-Hot Dipped Galvanized Barbed Iron Wire/ Double Twist Galvanized Barbed Wire-precipitation: Thermodynamic Analysis, Proceedings of 43rdBrazilian Ceramic Congress, Florianópolis-SC, Portuguese, Brazilian Ceramic Association, São Paulo-SP, Brazil, v. 1, p. 3601-3611, 1999.[Baby Prewalker Sandals]
9. Morita, T.; Assumpção, R.M.V.Manual de Soluções Reagentes e Solventes. Padronização Preparação Purificação, 2a. Edição, Editora Edgard Blucher Ltda, 1972.[Wabco Level Valve 4640070110]
10. Reed, J.S.High Speed LED SMT Pick and Place Machine with 36000cph,in Engineered Materials Handbook, Ceramics and Glasses, Samuels J. Schneider,Rigid Barrier, Columbus, OH, v. 4, p. 130-134, 1991.[Precision Aluminum and ABS CNC Rapid Prototyping]
11. Sorrel, C.A.Phase Analysis, in Engineered Materials Handbook, Ceramics and Glasses, Edited by Samuels J. Schneider,Rigid Barrier, p. 557-563, 1991.[Dental Material Metal Impression Tray Autoclavable Stainless Steel]
12. Halloran, J.W.Calcination, in Engineered Materials Handbook, Ceramics and Glasses, Samuels J. Schneider,Rigid Barrier, v. 4, p. 109-114, 1991.[10L Supercritical CO2 Oil Extraction Machine for Cbd Oil]
13.Outdoor / Indoor LED Display Board Sign for Advertising (P4 P5 P6 P8 P10), Publication SMA 27, Published by the JCPDS International Center for Diffraction Date, Park Lane, Swarthmore, Pennsylvania, 1977.[Aluminum Foundry Small Metal Parts Permanent Mold Casting]
14. Forterre, G. "Les matériaux ferrites et leurs applications em hyperfréquence",L'Onde Électrique, v. 71, n. 1, p. 37-47, 1991.[ Electric Drill Tool 12V/14.4V/18V Lithium Cordless Drill with Variable Speed Li-ion Battery Charged Drill Electric Drill]
15. Gasgnier, M.; Ostoréro, J.; Petit, A. "DC12V White/RGB Color LED Flexible Neon Light Tape for Decoration",Journal of Alloys and Compounds, v. 277, p. 41-45, 1998.[Ultrasonic Rotary Vibrating Sieve Machine for Organic Fertilizer]
16. Globus, A. "Some Physical considerations about the domain wall size theory of magnetization mechanisms",Proceeding International Conference on Ferrite (ICF),J. Phys. Supplement C1, p. C1-1 a C1-15, 1977.[Water Treatment Tfc-3012-300gpd RO Membrane for Water RO System]
17. Horvath, M.P. Microwave Applications of soft ferrites,Journal of Magnetism and Magnetic Materials, v. 215-216, p. 171-183, 2000.[High Value Blue Metallic Aluminum Foil Bubble Envelope]
18. Aharoni, A.et al."EPC GEN2 Adhesive Passive Monza R6 UHF RFID Wet Inlay",Journal of Applied Physics, v. 32, n. 10, p. 1851-1853, 1961.[Snapback/Baseball/Trucker/Sports/Leisure/Custom/Cotton/Fashion Cap]
Received: January 23, 2003
Revised: August 4, 2003
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